CH8281 Syllabus CHEMICAL ANALYSIS LABORATORY Regulation 2017 Anna University

CH8281 Syllabus OBJECTIVE

•  To make the student acquire practical skills in the wet chemical and \
  instrumentalmethods for quantitative estimation of nitrite in water, cement, oil, coal and Phenol.

CH8281 Syllabus LIST OF EXPERIMENTS

1. Determination of Redwood / Saybolt numbers, kinematic viscosity and viscosity index of Lubricating oils.

2. Determination of flash point, fire point, cloud and pour point of oils.

3. Determination of acid value and iodine value of oils.

4. Determination of COD of water samples.

5. Cement Analysis

a) Estimation of silica content

b) Estimation of mixed oxide content

c) Estimation of calcium oxide content

d) Estimation of calcium oxide by rapid method.

6. Coal Analysis a. Estimation of sulphur present in coal b. Ultimate analysis of coal c. Proximate analysis of coal.

7. Soap Analysis a. Estimation of total fatty acid b. Estimation of percentage alkali content.

8. Flue gas analysis by Orsat’s apparatus.

9. Estimation of phenol.

10. Determination of calorific value using bomb calorimeter.

11. Determination of nitrite in water.

CH8281 Syllabus Description of Equipment:

1. Silica Crucible 20 QTY

2. Heating Mantle 3 QTY

3. Muffle Furnace 1 QTY

4. Hot air oven 1 QTY

5. Desiccator 5 QTY

6. Vacuum Pump 1 QTY

7. Condenser 10 QTY

8. Reflux Condenser 10 QTY

9. Pensky martens closed cup apparatus 1 QTY

10. Cleveland Open cup apparatus 1 QTY

11. Cloud point apparatus 1 QTY

12. Saybolt Viscometer 1 QTY

13. Redwood Viscometer 1 QTY

14. Bomb Calorimeter 1 QTY

15. COD reflux 1 QTY

16. Orsat apparatus 1 QTY

17. UV-Vis Spectrophotometer 1 QTY

CH8281 Syllabus OUTCOME:

• Familiarization with equipment like viscometers, flash and fire point apparatus etc
• To familiarize of methods for determining COD
• Familiarization of a few simple synthetic techniques for soap

CH8281 Syllabus REFERENCES:

1. Environmental pollution analysis, S.M.Khopkar, New age international. 2011.

2. Manual of environmental analysis, N.C Aery, Ane books. 2010.

3. Text book of quantitative chemical analysis, J.Mendham, Pearson education 2008.

 

Subject Name	CHEMICAL ANALYSIS LABORATORY
Subject Code	CH8281
Regulation	2017
File	PDF
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Semester 2 Anna University Regulation 2017 Syllabus.

Syllabus for sem 2 Anna University Regulation 2017.